COSMETICS -
 FACE AND EYE MAKE UP REMOVER


1.       SCOPE AND FIELD OF APPLICATION
  This Gulf standard covers the requirements and specifications which must be met in cosmetics for face and eye make up remover.

2.       COMPLEMENTARY REFERENCES
2.1 Gulf Standard GSO 1943:2010 "Cosmetic products - Cosmetic Products Safety Requirements".

2.2 Gulf Standard GSO ISO 22716:2009 "Cosmetics - Good Manufacturing Practices (GMP) – Guidelines on Good Manufacturing Practices ".

2.3 Gulf Standard GSO ISO 22715:2008 "Cosmetics – Packaging and Labelling".

2.4 Gulf Standard GSO ISO 21148:2008 "Cosmetics - Microbiology – General Instructions for Microbiology Examinations".

2.5 Gulf Standard GSO ISO 18415:2009 "Cosmetics - Microbiology – Detection of Specified and Non-Specified Microorganisms".

2.6 Gulf Standard GSO ISO 18416:2009 "Cosmetics - Microbiology – Detection of Candida Albicans".

2.7 Gulf Standard GSO ISO 21149:2008 "Cosmetics - Microbiology – Enumeration and Detection of Aerobic Mesophilic Bacteria".

2.8 Gulf Standard GSO ISO 21150:2008 "Cosmetics - Microbiology – Detection of Escherichia Coli".

2.9 Gulf Standard GSO ISO 22717:2008 "Cosmetics - Microbiology – Detection of Pseudomonas Aeruginosa".

2.10 Gulf Standard GSO 917:1997 "Metal Aerosol Containers".

2.12 European Directives 76/768/EEC related to cosmetics, annexes and amendments.



3.       DEFINITIONS
For the purpose of this Standard the following terms and definitions shall have the meaning hereby assigned to them:
3.1 Face Make Up Remover Cosmetic: They are cosmtic products acting to remove face make up contents presented in creams and liquid emulsifiers, make up, loose and compact face powder and lip sticks.
3.2 Eye Make Up Remover Cosmetic: They are cosmetic products acting to remove eye make up presented in eyeliner pencils, eyebrows pencils, eyeshadow and mascara.
          LisRead phonetically
4.1 Face Make Up Remover Cosmetic
Existed in form of cream, liquid, oil, lotion or wetted tissues.

4.2 Eye Make Up Remover Cosmetic
Existed in form of oil, gel, lotion or wetted tissues.

5.       REQUIREMENTS
Face and eye make up remover cosmetics shall comply with the following requirements:
5.1 All contents and used preservative matter and colors shall be conforming according
Standards mentioned in sections (2.1, 2.12).
5.2 It shall pass all microbiological tests according to standards related to microbiological
Analysis and methods of testing for cosmetics which mentioned in sections (2.4, 2.5, 2.6, 2.7, 2.8, 2.9, 2.10) as below:
5.2.1 Free of fungus and yeasts.
5.2.2 Free of infectious bacteria.
5.3 It should not be causing any allergy for skin or eye.
5.4. It shall be free from rancidity.
5.5 It shall be removed easy by normal water.
5.6 It shall be removing all types of face and eye make up contents even waterproof type.

6.       SAMPLING 
6.1              The following shall be considered when taking samples:
6.1.1          Sampling shall be done in a clean dirt free environment.
6.1.2          The sampling instruments shall be clean and dry
6.1.3          Samples shall be kept in appropriate clean, dry and closed containers.
6.1.4           Each sample container shall be sealed in an airtight container and shall be kept at a temperature almost identical to the normal room temperature.
6.2           Allotment of Samples
6.2.1          Test representative sample has to be taken as tripartite one to be sent to laboratory, second to be kept with party that withdrew the sample and the third to be kept with withdrawn party.
Note: In case of small containers which is hard to write all required information, whole
Empty container has to be withdrawn along with sample withdrew container.

7.       TEST METHODS
7.1      Testing face and eye make up remover cosmetics test samples shall be carried out
In accordance with the Gulf standards and Global Standards mentioned in section (2) for
Complementrary references.
7.2 Isolation of fatty matter:
In case of existence of fatty matter, it has to be isolated first before carrying out rancidity test.
7.2.1 Instruments:
- Separation flask of 500 ml capacity
- Separation funnel of 500 ml capacity
- Beaker of 250 ml capacity
7.2.2 Used Solutions:
- Hydrochloric Acid (HCL) 10%
- Ethanol 95 %
- Petroleum Ether 40/60
7.2.3 Method:
7.2.3.1 An amount of 2-3 g of homogenized product shall be weighed in beaker 250 ml and added with 20 ml of ethanol, shaked well until entirely dissolved. Undirectly heating in water bath can be done with extra amount of alcohol if needed.
7.2.3.2 An amount of water to be added to beaker which is equivalent to volume of alcohol in
Sample. Sample then to be transferred to separation funnel of 500 ml capacity and beaker to
Be washed several times by 50 % ethanol.
7.2.3.3 Place 20 ml of HCL 10 % in separation funnel and shaked well, then leaving to stand
Until separation (isolation) of fatty acids in the upper layer.
7.2.3.4 An amount of 50 ml petroleum ether to be added, shaked the funnel well with
Evacuating the pressure, leaving until separation, then ether layer to be taken to another s
Separation funnel.
7.2.3.5 Ether lay to be washed with amount of 50 ml water containing of 50 % ethanol, ether
Layer to be separated in 200 ml beaker and evaporated in water bath.
Afterthat, the remained fatty matter in beaker to be taken and carried out rancidity test (chris
test).
7.3 Determination of Rancidity (Chris Test)
7.3.1 Instruments:
Clean and dry test tubes
7.3.2 Reagents:
- High purity Hydrochloric Acid (HCL) molecular weight 1.19
- 0.1% of floroglycinol solultion (0.1 g of floroglycinot dissolved in 100 ml diethyl ether)
7.3.3 Method:
7.3.3.1 An amount of 3 ml from fatty matter to be taken and placed in test tube. An amount of 5 ml of concentrated HCL to be added and shaked well (can be warmed). Then leaving it until cooling down, later 5 ml amount of floroglycinol solultion to be added.
If a crimson red color shows in the acidic lower layer, it means that it contains rancidity.

8.       PACKAGING, PACKING AND STORAGE
The following shall be taken into consideration at the time of packaging packing and storing
Face and eye make up remover cosmetics:
8.1 Product shall be packaged inside appropriately close covers in order to protect the the
Main ingredients and properties.
8.2   Product shall be packed inside appropriate containers as to ensure protection for them
From external influences, loss or damage during multiple shipments, transportation,
Handling and storage.
8.3 The containers shall be clean tightly closed.
8.4 The containers shall not affect or be affected by the product.
8.5 The product shall be stored in adequate conditions away from light and heat to ensure it r
Remains safe.
8.6 In case of using aeorosol containers (spray), it shall be conforming to gulf standard
Mentiond in section (2.11).

9.       LABELLING
The following information shall be stated clearly and legibly in Arabic or in both Arabic
And English on face and eye make up remover cosmetics containers and on the label as follows;
9.1 Name of the product.
9.2 Name of manufacturer, the address and/or his trademark.
9.3 Name of importer and the address in case of importing.
9.4 Date of production and Batch number.
9.5 Country of origin and if the product is manufactured under a registered trademark.
9.6 Net weight (g) or volume (ml).
9.7 Purpose of use.
9.8 Directions and instructions for method of use and storage conditions.
9.9 Shelf- life and validity.
9.10 Contents of concentration more than 1% should be written in descending order, however
Contents of concentration lower than 1% can be written without order.
9.11 Preservative matter, aromatic additives and colored matter with color number (if found).
9.12 Precautions and warnings should be taken into consideration when use (if found).
9.13 In case of mentioning any existence of additives, it has to match cosmetic actual
Contencts, and if additives were extracts, it has to clarify whether naturally (Extracted) or
Unnaturally (Flavored).
9.14 In case of mentioning that sample is free, it required at least the below informaion:
-        Name of manufacturer and address or name of importer and address in case of Importing.
-        Warning statements (if found).
-        Using instructions (if found).
10.     RULES FOR ACCEPTANCE AND REJECTION
10.1 Each consignment of face and eye make up remover cosmetics containers must be accompanied with a certificate issued either from National Standardization Body (NSB) or from any other official body approved by NSB showing that the consignment is complying with this gulf standard.
10.2 The consignment is considered complying if it the samples (Final sample representing
The consignment) have passed all the required tests analysis as stated in this Standard.
10.3 In case one or more samples failed any of the tests, a second sample twice the size of the
First sample shall be withdrawn from the same consignment and be subjected to all the
 Required tests. Other than that, the consignment shall be considered not complying with
This standard.
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Foreword

GCC Standardization Organization (GSO) is a regional Organization which consists of the National Standards Bodies of GCC member States. One of GSO main functions is to issue Gulf Standards /Technical regulations through specialized technical committees (TCs).

GSO through the technical program of committee TC No. 1 "Gulf TC of Chemical and Textile" has prepared the Gulf Standard No. :…. /2011 "Cosmetics-Face and Eye Make Up Remover ". The Draft Standard has been prepared by (United Arab Emirates).

This standard has been approved as a Gulf Technical Regulation by GSO Board of Directors in its meeting No.(       ),held on      /     /             H ,     /     /            G.


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